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The purified particles after drop-casting on glass were completely dried at room temperature, and then AFM micrographs were taken under frequency (300 kHz) in multimode SPM [27]

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The sequence parameters included a TE of 80 ms, TR of 2,000 ms, water suppression using a multiple optimized insensitive suppression train, pulse duration of 20 ms, an estimated water peak of 4.68 ppm, editing pulses interleaved at 1.9 ppm (ON) and 1.5 ppm (OFF), averaging two signals, a phase cycle of 16, frequency stabilization, and a total of 160 dynamic scans

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