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Samples were diluted 50 times with HPLC grade water and transferred to LC-MS glass vials for quantification on a Waters ACQUITY Xevo TQ-S UPLCMS/MS (Waters Corporation) under negative mode (ESI-)

If you've been at the treatment for 6 months and have lost less than 5% of your starting weight, then switching to an alternative medication may be medically advisable after discussing it with your prescriber

doi: 10.1038/s41590-020-00829-6 57 ZhangWHuangHCaiHTanWS